Indian Patents. 190905:A PROCESS FOR PREPARATION OF SAPINDUS TRIFOLIATUS BASED CLEANSER CUM CONDITIONER FOR HAIR

Title of Invention	A PROCESS FOR PREPARATION OF SAPINDUS TRIFOLIATUS BASED CLEANSER CUM CONDITIONER FOR HAIR
Abstract	1 A process for the extraction and preparation of formulation of hair cleanser and conditioner from the fresh or dried flesh of the Saplndus Trifoliate fruits, comprising the steps of. In sequence : subjecting the said flesh to extraction - step -1 bo form an extract further subjecting the said extract to formulation - step -2

Full Text	This invention relates to a process for preparation of Spends Trifoliate based hair cleanser cum conditioner. Hair cleansers cum conditioners of natural origin i,e, herbal origin are generally preferred to the synthetic ones because of their law toxicity to human beings; less harm to the body; and least side reactions and allergies to human beings in comparison to chemical cleansing agents, The Invention in general relates to Sapindus Trifoliate Extract generally known as Reeta Extract with long shelf and storage period and improved cleansing and conditioning efficacious. Sapindus Trifoliate is l PRIOR ART Direct application of Sapindus Trifoliate wet paste on the hair is likely to result in the deposition of high concentration on certain areas, rough handling and difficulty to perform the cleansing job and the washing off the paste from the head. The act is more tearful to the hair due to rough handling and simultaneously being difficult to collect fresh Spends Trifoliate each time just prior to the use. Therefore from the availability and safety point of view, fresh Sap Indus Trifbiiatus has to be collected, soaked over-night, tiioroughly and smoothly ground and mixed with water just prior to every use. But such aqueous paste is not known to have been used on a commercial scale as a cleanser due to factors such as unstable nature of the aqueous mixture over long periods of time. The paste develops malodor, discoloration due to biodegradation because of the presence of microbial and en2ymes. of extensive research and experiments it has been concluded and arrived at a Sapindus Trifbiiatus based hair cleanser which is storage stable, water scrubbed, safe and rich in cleansing ark corxlitioner principles. The prior art does not refer to stable Sapindus Trifoliate extract from natural resources containing the cleansing feature arxi conditioning feature to the hair-care product In so far as said preferences are absent; In the prior art, both the product of this invention, a series of Spends Trifoliate based extract and the hereinafter described process for the same are novel. It Is the object of the present Invention to full the lacunae existing in the prior art It is another object of the invention to arrive at an end product, whose quality Is better than the ones existing currently and is readily available off the shelf with a long shelf period. It is another object of the present invention towards making heri>ai and natural hair-care product In the context of present trends towards herbal cleansing agents, the importance of a product containing only natural resources cannot be overstressed. It is also significant to note that all the raw materials for Sapindus Trifbliatus based cleanser cum conditioner is renewable resource Accordingly another object of the present invention is to provide a process for the preparation of Saplndus Trifbliatus based conditioner which is storage stable, water soluble, safe and rich In hair cleansing and conditioner principles. It Is another object of the Invention to enhance cleansing efficacy by their use in formulated products. It is another object of the invention to entrance conditioning effect imparted by their use in formulated inflicts. These and other objects of the invention will be apparent from ensuing description. MAIN ADYANTAGES OF THE INVENTION Systematic Process for Extraction with higher extraction levee and more efficiently. Formulation consisting of naturally derived surfactant systems and ingredients to enhance cleansing and conditioning effect Systematic Process for the formulation to enhance stability and quality of the finished product Besides, the other advantages are : - ♦ Optimal extraction of herbal Ingredient's essence. ♦ Retention of natural fragrance of the herbal products formulated as above for imparting cleansing and conditioning and possibility of using/marketing these products with and without the use of additional perfume/s. Possibility of using surfactant system wherein all the ingredients are derived from natural renewable resources. Optimal/high level of incorporation of these herbal ingredients in the formulated produds. Use of thickening agents derived from natural renewable re¬sources. Improved rheologlcal properties of the final products having high level of these herbal ingredierrts. DESCRIPTION OF THE INVENTION According to this invention, the enhanced stability of the herbal extract in formulated product/s originates fix>m the controlled process of extraction which has been developed by the inventors. According to the inventiorv there is provided a process for the manufectunere of Sapindiis Trifoliatus based hali- cleanser cum condltJoner comprising : a. preparation of Sapindus THfoilatus extract b. preparation of preservative and stability fomuHatlon. c. mixing of Sapindies Trifoliatus extract with said the fomrujlatlon tD activate the d«sirad content of the final product Said preparation of Sapindus Trifoliatus extract comprising of steps of: - a. preparation of Sapindus Trifoliatus fiesh/pulp. b. crushing of Sapitxiu!; Trifoliatus flesh/pulp. c. filltration of Sapindus Trifoliatus pulp. Said preparation of preservation/stability formulation comprising of steps of:- a. Natural gum is dispersed in water to yield at 4% solution. b. Sapindus Trifoliatus Extract and water are mixed under a propeller stimar. The coconut fatty alcohol ethyoxylate sulphate sodium salt and fatty alcohol giucodise are added in the given order to the bulk under constant stirring. Preservative, perfume and coloring agents are added in that onier to the mass under constanc mixing. The above is mixed for 15 minutes. The pnxess Is now described herein below In its broadest scopes and aspect and the possible variant (Matures and characteristics c^ tfie invention are described along with equivalent fieature and characteristics in the preferred embodiment The preferred embotiment: is described herein below : - The preparation of Sapindus Trifbiiatus fruit comprises of depulping of removal of Sapindus Trifbiiatus seeds. While several different crushing/expelling means is adopted in tiie invention, the preferred means are crushing the fruits in crushers by manual crushing method. Water and several other ingredients were adopted for (brmulation of the Sapindus Trifollatus cleanser cum conditioner, in the invention In the preferred embodiment A natural gum derivative 4% solutions, coconut fatty alcohol-ethoxylate sutphonate sodium salt; coconut/palm fatty alcohoi-glucoslde; preservatives; sequestrant; natural proteins; quaterrdum salt; perfume. coloring agent and sterile delonlsed water and/or mixtures thereof are used for said formulations. A set sequence of said preferred ingredients and mixtures thereof having been workad out for optimum effect for the various stages of formulation In the preferred embodiment Said use of tt^ mixed Ingredients in said formication of Sapindus Trifoliatus paste is a novel development. in the interest of ooxin control, the preferred embodiment provides for treatment of said Sapindus Trifoliatus paste with preservative singly or in association with 2 or nrx^re such preservatives. Passing of the liot Sepifidus Trifoliatus paste through the filtration cloth is adopted in the preferred embodiment so as to facilitate the filtration process Stirring is carried out by agitation in the preferred embodiment The agitation is provided by stirrer propeller In the preferred embodiment The preferred ennbodiment also provides for stabilisation of the Sapindus Trifoliatus extract A furtlier treatment in the preferred embodiment, Is the use of naturally derived surfactant systems and special ingredients such as : sequestrant for reducing the harxiness of water; natural proteins for enrlcNng the scalp; quabemium salt for minimising the tangling of hair after wash; removal of bacteria from scalp and for reduction of dandruff on scalp and many more advantages. The invention is further illustrated by ttie preferred ennbodiment wNch Is now described in detail herein below. However, the scope of the invention Is not limited by said preferred embodiment SILECTIQW : Sapindus Trifoliatus fruits of a particular stage of ripeness which vary from green to dark brown color are collected and de-pulped in crcshers. The preferred appearance of the fruit is Pale Brown to Dark Brown cok}r with sNny pods. The preferred average weight of each pod is 4.0 to 5.10 gms. The preferr The pulp is separated and cut into pieces of uniform size between 5-10 mm size. CRUSHING : The pulp is then soaked in water in the ratio of one part by weight of pulp to 6 parts of water for 3-5 hours. The soaked wet pulp is then transferred into a round bottom flask for crushing the pulp into paste. REPLUXING : The flask has two hoted lid. Through the first hole, a pn^peiter surrer Is fixed and through the second hole, a reflux condenser is fixed. The pulp is agitated for 15 - 20 minutes in the flask by stirrer at 60 rpm at a temperature of 9095 C. The pulp is allowed to simmer. The temperotune is maintained between 90-95P C for 1/4 hour under constant agitation and relexing. Slowly the pulp is disintegrated and forms a thick paste. FILTERATION: This process is selected so as to provide the most economical and desired quality of the paste by the method of stirring and refluxing. The hot paste is then transferred for filtration through an non-woven nylon cloth (quality 1969). PBESERVATIVES : To prevent the deterioration of the smooth pasty filtrate, preservatives are then added. It Is again then stirred. The agitation and stirring Is done at room temperature. SEALING:The Sapindus Trifollatus paste with the preservative Is sent being Immediately for sealing In airtight containers. The storage In the airtight cxantalnens Is only for 20-24 hours before being sent for formulation. PARAMETER: The typical extract quality is as given below : - FORMULATION : The Sapindus Trifollatus paste treated with preservative is now is taken for further formulation to enhance storage stability and enhancing cleansing efficiency and conditioning effect At this stage, stabilisers, coloring agents, anomatic agerrts, arti-deteriorating agents; agents enhancing cleansing and conditioning; anti- blodegradatlon agents are added in a particular sequence as given below : {-) Saplndus Trifollatus extract 50% (-) natural gum is dispersed in water to yield a 4% solution 19% (-) 5apindi» Trifbliatus extract and the said water are transferred to the f!ask. (-) mixing of said Sapindus Trifbliatus extract and water is done by means of a propeller stirrer. (-) the Sapindus Trifbliatus paste is now thinned for further processlng. (-) the thin paste is kept under constant stirring and mixing. (-) at this stage : - (-) coconut fatty alcohol ethoxylate suplhorate sodium salt 6% (-) preservatives (Phenoxyethanol, Methyl Paraben, Propyl Paraben). 0.5 (-) fatty alcohol glucoside 2% (-) sequ«strant (Khylenedlamine, Tetraacteic Acid Disodium Salt) 0.05P/O (-) natural proteins qs (-) Quatemium Salt qs (-) perfume qs (») coloring agents (Chocolate Brown) qs (-) sterile deiodised water qs - ICX) is added in sequence as mentioned herein above, under connstant: stirring. The above composition is mixed for 15 minutxas. As discribed here in above, the above formulation so prepared is capable of storrage for minimum period of one year without any degradation or loss of cleansing/conditioning efficacies as compared to the regular home made Sapindus Trifoliatus Extract The formulation as has been made with the judicious adjustments of levels of speciality ingredients which are natural, is capable of giving an Improved cleansing and conditioning efficacies. As described herein above, the above formulation is to be prepared by a certain sequential addition of various ingredients, in the medium of water, to arrive at the finished product with prolonged storage in respect of stability and with improved cleansing and conditioning efncacies. WE CLAIM;- 1 A process for the extraction and preparation of formulation of hair cleanser and conditioner from the fresh or dried flesh of the Saplndus Trifoliate fruits, comprising the steps of. In sequence : subjecting the said flesh to extraction - step -1 bo form an extract further subjecting the said extract to formulation - step -2 WHEREIN SAID Extractor - STB'- 1 AEAAG; - a. subjecting the said flesh to cutting and sizing them to pieces of 5- 10 mm size ; b. adding water in the ratio of one part by weight of flesh to 6 parts of water; c. soiling the flesh for 3-5 hours ; d. transferring the wet soaked flesh into a round bottom flask kept at temperature of 90 - 95 C ; e. stirring the wet soaked flesh through a propeller stirrer fixed in the first hole of the said flask until simmering to form a crude mix ; f. refluxing the crude mix through a reflux condenser flexed in the second hole of the said flask, for 15-20 minutes to form a crude extract; g. filtration of crude extract through a filter consisting of non-woven nylon cloth to form the filtrate ; h. addition of known preservatives to the filtrate ; I. mixing of the preservatives to the filtrate thoroughly by means of stirrer to obtain a uniform extract; j. cooling of the uniform extract to room temperature ; k. storing for less than 24 hours of the unionism extract in an air tight container for use In formulation. //. WHEREIN SAID FORMULATION STEP - 2 MEANS :- and process of adding the above mentioned ingredients one by one in sequence to a container. Z The proess of claim 1, wherein step (a), (b) and (c) is repeated a piuraiity of times, each with a new batch of flesh, to provide a plurality of batches, said batches being combined and concentrated to form a thick syrup. 3. The process of claim 1, wherein step (d), the flask consists of round bottom and fitted with a (id having two holes. One hole being in the centre of the lid and the second hole a little distance away from the centre. In the said centre hole, a propeller stirrer Is fixed. In the second hole, a condenser is fixed. The temperature of the flask is maintained between 90-95f C. 4. The process of claim 1, wherein step (e) the wet soaked flesh is kept under gentle agitation by stirring with the propeller stirrer at 60 rpm to form a uniform smooth crude mix. 5. The process of claim 1, wherein step (f), the saki crude mix of the said wet soaked flesh Is heated to simmering. It is then allowed to Simmer for 15-20 minutes at a temperature of 90 - 95 C under constant agitation and refluxlng to form a crude extract 6. The process of claim 1, wherein step (g), the crude extract is ftltanod through a nan-vmven cloth, to obtain a snrwoth clean Sapindus Trlfbliatus paste as filtnite. 7. The process of claim 1, wherein step (h) and (i) the preservatives used to the filtrate are a single preservative or group of associated preservative to effect the stability of the extract. a The process of claim 1, wherein step (J), the extract; consisting of said extract with the preservative is transferred to a clean, dry, air tight containers and stored for a period of 10-24 hours until formulation.

Full Text

This invention relates to a process for preparation of Spends Trifoliate based hair cleanser cum conditioner. Hair cleansers cum conditioners of natural origin i,e, herbal origin are generally preferred to the synthetic ones because of their law toxicity to human beings; less harm to the body; and least side reactions and allergies to human beings in comparison to chemical cleansing agents,
The Invention in general relates to Sapindus Trifoliate Extract generally known as Reeta Extract with long shelf and storage period and improved cleansing and conditioning efficacious. Sapindus Trifoliate is l PRIOR ART
Direct application of Sapindus Trifoliate wet paste on the hair is likely to result in the deposition of high concentration on certain areas,

rough handling and difficulty to perform the cleansing job and the washing off the paste from the head. The act is more tearful to the hair due to rough handling and simultaneously being difficult to collect fresh Spends Trifoliate each time just prior to the use. Therefore from the availability and safety point of view, fresh Sap Indus Trifbiiatus has to be collected, soaked over-night, tiioroughly and smoothly ground and mixed with water just prior to every use. But such aqueous paste is not known to have been used on a commercial scale as a cleanser due to factors such as unstable nature of the aqueous mixture over long periods of time. The paste develops malodor, discoloration due to biodegradation because of the presence of microbial and en2ymes.
of extensive research and experiments it has been concluded and arrived at a Sapindus Trifbiiatus based hair cleanser which is storage stable, water scrubbed, safe and rich in cleansing ark corxlitioner principles.
The prior art does not refer to stable Sapindus Trifoliate extract from natural resources containing the cleansing feature arxi conditioning feature to the hair-care product

In so far as said preferences are absent; In the prior art, both the product of this invention, a series of Spends Trifoliate based extract and the hereinafter described process for the same are novel.
It Is the object of the present Invention to full the lacunae existing in the prior art
It is another object of the invention to arrive at an end product, whose quality Is better than the ones existing currently and is readily available off the shelf with a long shelf period.
It is another object of the present invention towards making heri>ai and natural hair-care product In the context of present trends towards herbal cleansing agents, the importance of a product containing only natural resources cannot be overstressed. It is also significant to note that all the raw materials for Sapindus Trifbliatus based cleanser cum conditioner is renewable resource
Accordingly another object of the present invention is to provide a process for the preparation of Saplndus Trifbliatus based conditioner which is storage stable, water soluble, safe and rich In hair cleansing and conditioner principles.

It Is another object of the Invention to enhance cleansing efficacy by their use in formulated products.
It is another object of the invention to entrance conditioning effect imparted by their use in formulated inflicts. These and other objects of the invention will be apparent from ensuing description.
MAIN ADYANTAGES OF THE INVENTION
Systematic Process for Extraction with higher extraction levee and more efficiently.
Formulation consisting of naturally derived surfactant systems and ingredients to enhance cleansing and conditioning effect
Systematic Process for the formulation to enhance stability and quality of the finished product
Besides, the other advantages are : -
♦ Optimal extraction of herbal Ingredient's essence.

♦ Retention of natural fragrance of the herbal products formulated as above for imparting cleansing and conditioning and possibility of using/marketing these products with and without the use of additional perfume/s.
Possibility of using surfactant system wherein all the ingredients are derived from natural renewable resources.
Optimal/high level of incorporation of these herbal ingredients in the formulated produds.
Use of thickening agents derived from natural renewable re¬sources.
Improved rheologlcal properties of the final products having high level of these herbal ingredierrts.
DESCRIPTION OF THE INVENTION
According to this invention, the enhanced stability of the herbal extract in formulated product/s originates fix>m the controlled process of extraction which has been developed by the inventors.

According to the inventiorv there is provided a process for the manufectunere of Sapindiis Trifoliatus based hali- cleanser cum condltJoner comprising :
a. preparation of Sapindus THfoilatus extract
b. preparation of preservative and stability fomuHatlon.
c. mixing of Sapindies Trifoliatus extract with said the fomrujlatlon
tD activate the d«sirad content of the final product
Said preparation of Sapindus Trifoliatus extract comprising of steps of: -
a. preparation of Sapindus Trifoliatus fiesh/pulp.
b. crushing of Sapitxiu!; Trifoliatus flesh/pulp.
c. filltration of Sapindus Trifoliatus pulp.
Said preparation of preservation/stability formulation comprising of steps of:-
a. Natural gum is dispersed in water to yield at 4% solution.
b. Sapindus Trifoliatus Extract and water are mixed under a
propeller stimar. The coconut fatty alcohol ethyoxylate sulphate
sodium salt and fatty alcohol giucodise are added in the given

order to the bulk under constant stirring. Preservative, perfume and coloring agents are added in that onier to the mass under constanc mixing. The above is mixed for 15 minutes.
The pnxess Is now described herein below In its broadest scopes and aspect and the possible variant (Matures and characteristics c^ tfie invention are described along with equivalent fieature and characteristics in the preferred embodiment
The preferred embotiment: is described herein below : -
The preparation of Sapindus Trifbiiatus fruit comprises of depulping of removal of Sapindus Trifbiiatus seeds. While several different crushing/expelling means is adopted in tiie invention, the preferred means are crushing the fruits in crushers by manual crushing method. Water and several other ingredients were adopted for (brmulation of the Sapindus Trifollatus cleanser cum conditioner, in the invention In the preferred embodiment
A natural gum derivative 4% solutions, coconut fatty alcohol-ethoxylate sutphonate sodium salt; coconut/palm fatty alcohoi-glucoslde; preservatives; sequestrant; natural proteins; quaterrdum salt; perfume.

coloring agent and sterile delonlsed water and/or mixtures thereof are used for said formulations. A set sequence of said preferred ingredients and mixtures thereof having been workad out for optimum effect for the various stages of formulation In the preferred embodiment
Said use of tt^ mixed Ingredients in said formication of Sapindus Trifoliatus paste is a novel development.
in the interest of ooxin control, the preferred embodiment provides for treatment of said Sapindus Trifoliatus paste with preservative singly or in association with 2 or nrx^re such preservatives.
Passing of the liot Sepifidus Trifoliatus paste through the filtration cloth is adopted in the preferred embodiment so as to facilitate the filtration process
Stirring is carried out by agitation in the preferred embodiment The agitation is provided by stirrer propeller In the preferred embodiment
The preferred ennbodiment also provides for stabilisation of the Sapindus Trifoliatus extract

A furtlier treatment in the preferred embodiment, Is the use of naturally derived surfactant systems and special ingredients such as : sequestrant for reducing the harxiness of water; natural proteins for enrlcNng the scalp; quabemium salt for minimising the tangling of hair after wash; removal of bacteria from scalp and for reduction of dandruff on scalp and many more advantages.
The invention is further illustrated by ttie preferred ennbodiment wNch Is now described in detail herein below. However, the scope of the invention Is not limited by said preferred embodiment
SILECTIQW : Sapindus Trifoliatus fruits of a particular stage of ripeness which vary from green to dark brown color are collected and de-pulped in crcshers. The preferred appearance of the fruit is Pale Brown to Dark Brown cok}r with sNny pods. The preferred average weight of each pod is 4.0 to 5.10 gms. The preferr The pulp is separated and cut into pieces of uniform size between 5-10 mm size.

CRUSHING : The pulp is then soaked in water in the ratio of one part by weight of pulp to 6 parts of water for 3-5 hours. The soaked wet pulp is then transferred into a round bottom flask for crushing the pulp into paste.
REPLUXING : The flask has two hoted lid. Through the first hole, a pn^peiter surrer Is fixed and through the second hole, a reflux condenser is fixed. The pulp is agitated for 15 - 20 minutes in the flask by stirrer at 60 rpm at a temperature of 9095 C. The pulp is allowed to simmer. The temperotune is maintained between 90-95P C for 1/4 hour under constant agitation and relexing. Slowly the pulp is disintegrated and forms a thick paste.
FILTERATION: This process is selected so as to provide the most economical and desired quality of the paste by the method of stirring and refluxing. The hot paste is then transferred for filtration through an non-woven nylon cloth (quality 1969).
PBESERVATIVES : To prevent the deterioration of the smooth pasty filtrate, preservatives are then added. It Is again then stirred. The agitation and stirring Is done at room temperature.

SEALING:The Sapindus Trifollatus paste with the preservative Is sent being Immediately for sealing In airtight containers.
The storage In the airtight cxantalnens Is only for 20-24 hours before being sent for formulation.
PARAMETER: The typical extract quality is as given below : -

FORMULATION : The Sapindus Trifollatus paste treated with preservative is now is taken for further formulation to enhance storage stability and enhancing cleansing efficiency and conditioning effect
At this stage, stabilisers, coloring agents, anomatic agerrts, arti-deteriorating agents; agents enhancing cleansing and conditioning; anti-

blodegradatlon agents are added in a particular sequence as given below :
{-) Saplndus Trifollatus extract 50%
(-) natural gum is dispersed in water to yield a 4% solution 19%
(-) 5apindi» Trifbliatus extract and the said water are transferred to the f!ask.
(-) mixing of said Sapindus Trifbliatus extract and water is done by means of a propeller stirrer.
(-) the Sapindus Trifbliatus paste is now thinned for further processlng.
(-) the thin paste is kept under constant stirring and mixing.
(-) at this stage : -
(-) coconut fatty alcohol ethoxylate suplhorate sodium salt 6%
(-) preservatives (Phenoxyethanol, Methyl Paraben, Propyl Paraben). 0.5
(-) fatty alcohol glucoside 2%
(-) sequ«strant (Khylenedlamine, Tetraacteic Acid Disodium Salt) 0.05P/O
(-) natural proteins qs
(-) Quatemium Salt qs
(-) perfume qs
(») coloring agents (Chocolate Brown) qs
(-) sterile deiodised water qs - ICX)

is added in sequence as mentioned herein above, under connstant: stirring. The above composition is mixed for 15 minutxas.
As discribed here in above, the above formulation so prepared is capable of storrage for minimum period of one year without any degradation or loss of cleansing/conditioning efficacies as compared to the regular home made Sapindus Trifoliatus Extract The formulation as has been made with the judicious adjustments of levels of speciality ingredients which are natural, is capable of giving an Improved cleansing and conditioning efficacies.
As described herein above, the above formulation is to be prepared by a certain sequential addition of various ingredients, in the medium of water, to arrive at the finished product with prolonged storage in respect of stability and with improved cleansing and conditioning efncacies.

WE CLAIM;-
1 A process for the extraction and preparation of formulation of hair cleanser and conditioner from the fresh or dried flesh of the Saplndus Trifoliate fruits, comprising the steps of. In sequence :
subjecting the said flesh to extraction - step -1 bo form an extract further subjecting the said extract to formulation - step -2
WHEREIN SAID Extractor - STB'- 1 AEAAG; -
a. subjecting the said flesh to cutting and sizing them to pieces of 5-
10 mm size ;
b. adding water in the ratio of one part by weight of flesh to 6 parts
of water;
c. soiling the flesh for 3-5 hours ;
d. transferring the wet soaked flesh into a round bottom flask kept at
temperature of 90 - 95 C ;
e. stirring the wet soaked flesh through a propeller stirrer fixed in the
first hole of the said flask until simmering to form a crude mix ;
f. refluxing the crude mix through a reflux condenser flexed in the
second hole of the said flask, for 15-20 minutes to form a crude
extract;

g. filtration of crude extract through a filter consisting of non-woven
nylon cloth to form the filtrate ; h. addition of known preservatives to the filtrate ; I. mixing of the preservatives to the filtrate thoroughly by means of
stirrer to obtain a uniform extract;
j. cooling of the uniform extract to room temperature ;
k. storing for less than 24 hours of the unionism extract in an air tight
container for use In formulation.
//. WHEREIN SAID FORMULATION STEP - 2 MEANS :-

and process of adding the above mentioned ingredients one by one in sequence to a container.
Z The proess of claim 1, wherein step (a), (b) and (c) is repeated a piuraiity of times, each with a new batch of flesh, to provide a plurality of batches, said batches being combined and concentrated to form a thick syrup.
3. The process of claim 1, wherein step (d), the flask consists of round bottom and fitted with a (id having two holes. One hole being in the centre of the lid and the second hole a little distance away from the centre. In the said centre hole, a propeller stirrer Is fixed. In the second hole, a condenser is fixed. The temperature of the flask is maintained between 90-95f C.
4. The process of claim 1, wherein step (e) the wet soaked flesh is kept under gentle agitation by stirring with the propeller stirrer at 60 rpm to form a uniform smooth crude mix.
5. The process of claim 1, wherein step (f), the saki crude mix of the said wet soaked flesh Is heated to simmering. It is then allowed to Simmer for 15-20 minutes at a temperature of 90 - 95 C under constant

agitation and refluxlng to form a crude extract
6. The process of claim 1, wherein step (g), the crude extract is
ftltanod through a nan-vmven cloth, to obtain a snrwoth clean Sapindus
Trlfbliatus paste as filtnite.
7. The process of claim 1, wherein step (h) and (i) the preservatives
used to the filtrate are a single preservative or group of associated
preservative to effect the stability of the extract.
a The process of claim 1, wherein step (J), the extract; consisting of said extract with the preservative is transferred to a clean, dry, air tight containers and stored for a period of 10-24 hours until formulation.

Documents:

0878-mas-1999 claims.pdf

0878-mas-1999 correspondence-others.pdf

0878-mas-1999 description(complete).pdf

0878-mas-1999 form-1.pdf

0878-mas-1999 form-26.pdf

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Patent Number

190905

Indian Patent Application Number

878/MAS/1999

PG Journal Number

30/2009

Publication Date

24-Jul-2009

Grant Date

08-Mar-2004

Date of Filing

06-Sep-1999

Name of Patentee

M/S. CAVINKARE LIMITED

Applicant Address

NO.130, PETERS ROAD, CHENNAI 600 082

Inventors:

#	Inventor's Name	Inventor's Address
1	CHINI KRISHNAN RANGANATHAN	NO.130, PETERS ROAD, CHENNAI 600 086
2	VAIDYANATHA SWAMY RAMASUBRAMANIAN	NO.130, PETERS ROAD, CHENNAI 600 086
3	LAKSHMI THIAGARAJAN	NO.130, PETERS ROAD, CHENNAI 600 086

PCT International Classification Number

A61K 7/075

PCT International Application Number

N/A

PCT International Filing date

PCT Conventions:

#	PCT Application Number	Date of Convention	Priority Country
1			NA